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Item Thermal energy storage with sensible heat in an air-alumina packed bed using axial flow, axial flow with layers and radial flow(Montana State University - Bozeman, College of Engineering, 2020) Al-Azawii, Mohammad Mahdie Saleh; Chairperson, Graduate Committee: Ryan Anderson; Carter Theade, Megan Danczyk, Erick Johnson and Ryan Anderson were co-authors of the article, 'Experimental study on cyclic behavior of thermal energy storage in an air-alumina packed bed' published in the journal 'Journal of energy storage' which is contained within this dissertation.; Carter Theade, Pablo Bueno and Ryan Anderson were co-authors of the article, 'Experimental study of layered thermal energy storage in an air-alumina packed bed using axial pipe injections' in the journal 'Applied energy' which is contained within this dissertation.; Duncan Jacobsen, Pablo Bueno and Ryan Anderson were co-authors of the article, 'Experimental study of thermal behavior during charging in thermal energy storage packed bed using radial pipe' in the journal 'Applied thermal engineering' which is contained within this dissertation.Thermal behavior in a packed bed thermal energy storage (TES) system is studied experimentally. TES systems are a promising solution to integrate renewable energy sources such as solar energy. The performance of such systems can be affected by different variables such as storage material size/type, pressure, temperature, heat transfer fluid (HTF), storage type (sensible/latent heat), and flow rate. Although these variables have been studied in literature, the resulting thermal dispersion and heat losses to the environment have been considered in few studies. This thesis studies the thermal behavior of an air-alumina TES packed bed focusing on dispersion and heat losses to quantify the thermal performance. Reducing their effects can improve the thermocline and thus thermal efficiency. The research efforts in this work quantify these effects and provide two new methods to reduce thermal dispersion and increase exergetic efficiency. Three configurations were considered in the present study. In the first configuration, a traditional packed bed is used focusing on performance for multiple partial cycles. This configuration quantified the thermal performance and served as a basis to compare the results from the other configurations. Dispersion effects were found to accumulate before a steady state was achieved during cycling. In the second and third configurations, novel pipe injection techniques were used to charge/discharge the bed. First, the normal bed is divided into layers via inserting pipes along the bed's axial length, focusing on a full charge-discharge cycle. Results show that exergy efficiency increases with flow rate and number of layers. The thermocline improved and dispersion losses decreased with number of layers. Second, a perforated pipe to facilitate radial flow was inserted at the center of the bed along the axial length to heat the bed. Radial charging shows higher charging efficiency compared to normal axial charging. Pipe injection is a novel method and a promising technique that improves the thermal performance of a lab scale storage bed, especially the layering method. Radial injection warrants more investigation to quantify its performance in thermal cycles.Item An acoustic emission and hygrothermal aging study of fiber reinforced polymer composites(Montana State University - Bozeman, College of Engineering, 2019) Newhouse, Kai Jeffrey; Chairperson, Graduate Committee: David A. MillerFiber reinforced polymer matrix composites are a premier choice for offshore wind turbines and Marine Hydro-Kinetic Devices, which operate in harsh and isolated marine environments. These factors combined with decades long target service life make imperative the understanding of damage mechanisms and the environmental effects thereof. Acoustic emission monitoring is a research technology that uses specialized sensors to detect transient elastic waves in a material which originate from damage sources. Waveform parameters have been correlated with different damage mechanisms in fibrous composites. A diverse set of fiber-matrix combinations configured into a variety of layups totaling more than 30 laminates were mechanically tested in quasi-static uniaxial tension while monitoring acoustic emission. A subset of these materials was aged prior to testing in an artificial marine environment by soaking in a water bath of simulated seawater at 50 degrees Celsius. Various acoustic emission waveform parameters were investigated with respect to expected damage between layups and possible material-based differences. Among the conditioned material set, mechanical changes from moisture absorption shows mixed levels of degradation among different material systems. Moduli were generally unaffected with a few minor decreases. Strengths were reduced by as much as 41%, and failure strains fell as much as 47%. From acoustic emission investigation, good correlation is found between Fast Fourier Transform peak spectral frequency bands and expected damage mechanisms between layups. Material based peak frequency differences are found exclusively in interphase failures (de-bond and fiber pullout). Layup-based correlations in conjunction with elastic wave theory were used to put forth new frequency band ranges associated with damage types.Item Developments in electrically conductive bio-composites for use in additive manufacturing(Montana State University - Bozeman, College of Engineering, 2019) Arroyo, Jesse Whitney; Chairperson, Graduate Committee: Cecily Ryan; Cecily Ryan was a co-author of the article, 'Incorporation of carbon nanofillers tunes mechanical and electrical percolation in PHBV:PLA blends' in the journal 'Polymers' which is contained within this thesis.With the growth of rapid production methods, such as additive manufacturing, petroleum derived plastics are becoming ever more prevalent in consumer homes and landfills. As the industry grows, research into a more circular approach to designing and using materials is critical to maintaining sustainability. Bioplastics such as poly(hydroxybutyrate-co-hydroxyvalerate) (PHBV) and poly(lactic acid) (PLA) provide material properties comparable to petroleum derived plastics and are becoming more common in the additive manufacturing field. Biobased fillers, such as bio-derived cellulose, lignin byproducts, and biochar, can be used to modify the thermal, mechanical, and electrical properties of polymer composites. Biochar (BioC), in particular, is of interest for enhancing thermal and electrical conductivities in composites, and can potentially serve as a bio-derived graphitic carbon alternative for certain composite applications. In this work, we investigate a blended biopolymer system: PLA/PHBV, and addition of carbon black (CB), a commonly used functional filler as a comparison for Kraft lignin-derived BioC. We present calculations and experimental results for phase-separation and nanofiller phase affinity in this system, indicating that the CB localizes in the PHBV phase of the immiscible PHBV:PLA blends. The addition of BioC led to a deleterious reaction with the biopolymers, as indicated by blend morphology, differential scanning calorimetry showing significant melting peak reduction for the PLA phase, and a reduction in melt viscosity. For the CB nanofilled composites, electrical conductivity and dynamic mechanical analysis supported the ability to use phase separation in these blends to tune the percolation of mechanical and electrical properties, with a minimum percolation threshold found for the 80:20 blends of 1.6 wt.% CB. At 2% BioC (approximately the percolation threshold for CB), the 80:20 BioC nanocomposites had a resistance of 3.43x10 8 Omega as compared to 2.99x10 8 Omega for the CB, indicating that BioC could potentially perform comparably to CB as a conductive nanofiller if the processing challenges can be overcome. Investigations into alkaline and dealkaline lignin sources have shown that alkaline lignin experiences a significant effect on the thermal stability of PHBV eluding that alternate sources of lignin may provide a solution to the processing challenges mentioned. This work has helped to develop a understanding of the factors that aid in creating sustainable materials sourced from PLA,PHBV, and BioC.