Theses and Dissertations at Montana State University (MSU)

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    An experimental study of drying in porous media in novel 2D micromodels with dual porosity
    (Montana State University - Bozeman, College of Engineering, 2024) Habib, Md Ahsan; Chairperson, Graduate Committee: Yaofa Li
    Drying of porous media is pervasive in numerous natural and engineering processes, such as oil recovery, CO 2 storage, and critical zone science. Drying is essentially a multiphase flow process, where the liquid phase evaporates and is displaced/replaced by the gaseous phases, as vapor diffuses out of the porous structure. In terms of pore structure and other physical characteristics like porosity and permeability, many porous matrices exhibit multi-scale heterogeneity. For instance, in critical zone, soil is often viewed as a hierarchical organization: primary particles form aggregates, which in turn form macroaggregates, effectively leading to a dual-porosity medium. Numerous activities, including gases and water transport, are known to be controlled by the resultant multiscale flow dynamics and inter-/intra-aggregate interaction during drying. However, the fundamental physics underlying drying of porous media with dual porosity is not well understood from a fluid mechanics perspective. In this work, a novel 2D microfluidic device fabrication technique has been developed. To study the multi-phase flow of air and water, emphasizing the multi-scale interaction, pore structure, and role of film flows, three distinct types of microfluidic devices have been fabricated, which bear the innovative three-layer glass-silicon- glass architecture, providing precise structural control and excellent optical access from both top and bottom. An innovative dual-magnification imaging technique has been introduced adapted for micro-PIV and epi-fluorescent microscopy which offers insightful information about the flow dynamics at both the micro- and macro-scales concurrently. In this thesis, two distinct types of experiments are outlined, focusing on diffusion-driven drying and flow-through drying, utilizing three diverse micromodels characterized by varying porous structures and distributions. The experimental results have presented the overall drying dynamics observed in different micromodels, each featuring unique porous configurations. The impact of porous geometry and external flow conditions on drying rate and associated pore-scale physics is thoroughly examined. The findings encompass a comprehensive overview of micro-macro pore interactions, as evidenced by separated saturation distribution, displacement rates, and other pertinent flow parameters. The findings have reflected the influence of pore geometry, distribution, hydraulic connectivity, and film flow on the observed effects.
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    Nanocomposites : a study of theoretical micromechanical behavior using finite element analysis
    (Montana State University - Bozeman, College of Engineering, 2009) Milliren, Eric Carlton; Chairperson, Graduate Committee: Christopher H. M. Jenkins
    Current research in nanotechnology has produced an increasing number of possibilities for advanced materials. Among those materials with potential advanced mechanical properties are fiber-reinforced composite laminates that utilize nanoscale fiber diameters. Through a combination of studying classic micromechanical models and modern computer-aided finite element analysis (FEA), the advantages for utilizing these nanofibers in advanced structural applications, such as space mirror backings, was investigated. The approach for modeling these composite structures was that of a Representative Volume Element (RVE). Using the program ABAQUS/CAE, a RVE was created with the goals of accurately comparing to the shear lag theory, effectively incorporating "interphase" zones that bond the constituents, and demonstrating effects of down-scaling fiber diameter. In this thesis, the progression of the ABAQUS model is thoroughly covered as it developed into a verified model correlating with the shear lag theory. The model produced was capable of utilizing interphase if desired, and was capable of off-axis loading scenarios. A MathCAD program was written in order to employ the published theoretical techniques, which were then compared to the FEA results for verification. The FEA model was found to work well in conjunction with the theory explored using MathCAD, after which the nanofiber FEA model showed some clear advantages over a conventional-sized model, specifically an increase in strength of the composite RVE. Finally, it was determined that the interfacial bonding strength plays a large role in the structure of the interphase zone, and thus the overall strength of the composite.
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