Theses and Dissertations at Montana State University (MSU)

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    Resistance temperature devices fabricated using micro electromechanical systems technology designed and characterized for low-temperature applications
    (Montana State University - Bozeman, College of Engineering, 2020) Thomae, Madelyn Ruth; Chairperson, Graduate Committee: Stephan Warnat
    Research shows that microorganisms play a major role in climate change, but there is a lack of adequate understanding of microbial involvement in climate change and further research is needed for greater understanding. Temperature monitoring lends an insight into the current climatic shifts in Arctic and Antarctic regions. Currently, satellite monitoring is used to track temperature changes in those regions. To further the understanding of the role microorganisms play in the rising temperatures in those regions, in-situ temperature monitoring is needed. Commercially available temperature probes are high in cost and not well-suited for the harsh environment of Arctic and Antarctic regions. Utilizing micro electromechanical systems technology provides a solution for robust low-cost, low-power sensors that can be designed specifically to operate in harsh environments. Gold resistance temperature devices were designed and fabricated using micro electromechanical systems technology with a high spatial resolution capable of detecting microorganisms in subzero applications. The fabricated temperature sensors were calibrated for subzero use and freezing experiments were done to detect any changes due to impurities in the sample. The gold resistance temperature devices were able to withstand prolonged exposure to the harsh experimental environment and provide an accurate spatial temperature gradient throughout the media. The gold resistance temperature devices had negligible effects due to the self-heating phenomenon common in resistance temperature devices. Additionally, the sensors were able to detect variations in the freezing curve of the media with the inclusion of the bacterial isolate Flavobacterium sp. ANT 11 (accession number GU592435) in DI water samples. Future research should focus on (1) furthering the understanding of the microbial interactions in the cooling curves of different medias and (2) integrating electrical impedance spectroscopy sensors to provide knowledge of what impurities are in the sample that could be affecting the freezing curve of the media.
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    MEMS 3-dimensional scanner with SU-8 flexures for a handheld confocal microscope
    (Montana State University - Bozeman, College of Engineering, 2018) Liu, Tianbo; Chairperson, Graduate Committee: David Dickensheets
    The conventional method for diagnosing skin cancer is to perform a biopsy followed by pathology. However not only are biopsies invasive and likely to leave permanent scarring, they also sample the body sparsely. Fortunately, a non-invasive method of imaging called confocal laser scanning microscopy has shown great potential to replacing invasive biopsies. Confocal microscopy can use light to achieve high-resolution imaging of cells that lie underneath the surface of the skin. However, the large size of current confocal microscopes limits their application to all but the most accessible sites. In this dissertation, I address the miniaturization of confocal microscopy through the development of a new microelectromechanical systems scan mirror that can scan a focused beam in three dimensions. The scanner has a 4 mm aperture, and has the capability to replace all of the bulky beam scanners and focus mechanisms that contribute to the large size of current confocal microscopes. The fabrication of the scanner explores the use of the polymer SU-8 for its mechanical structures. The gimbal mirror has demonstrated scan angles in excess of plus or minus 3° mechanical for lateral scanning, and its deformable surface provided controllable deflection up to 10 microns for focus control. This newly developed scanner was integrated into a confocal system to test its imaging capabilities. The device demonstrated high-resolution scanning with simultaneous focus adjustment suitable for the next generation of miniaturized confocal laser scanning microscopes.
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    Imaging performance of elliptical-boundary varifocal mirrors in active optical systems
    (Montana State University - Bozeman, College of Engineering, 2015) Lukes, Sarah Jane; Chairperson, Graduate Committee: David L. Dickensheets
    Micro-electro-mechanical systems deformable-membrane mirrors provide a means of focus control and attendant spherical aberration correction for miniaturized imaging systems. The technology has greatly advanced in the last decade, thereby extending their focal range capabilities. This dissertation describes a novel SU-8 2002 silicon-on-insulator wafer deformable mirror. A 4.000 mm x 5.657 mm mirror for 45° incident light rays achieves 22 micron stroke or 65 diopters, limited by snapdown. The mirrors show excellent optical quality while flat. Most have peak-to-valley difference of less than 150 nm and root-mean-square less than 25 nm. The process proves simple, only requiring a silicon-on-insulator wafer, SU-8 2002, and a metal layer. Xenon difluoride etches the silicon to release the mirrors. Greater than 90% of the devices survive fabrication and release. While current literature includes several aberration analyses on static mirrors, analyses that incorporate the dynamic nature of these mirrors do not exist. Optical designers may have a choice between deformable mirrors and other types of varifocal mirrors or lenses. Furthermore, a dynamic mirror at an incidence angle other than normal may be desired due to space limitations or for higher throughput (normal incidence requires a beam splitter). This dissertation presents an analysis based on the characteristic function of the system. It provides 2nd and 3rd order aberration coefficients in terms of dynamic focus range and base ray incidence angle. These afford an understanding of the significance of different types of aberrations. Root-mean-square and Strehl calculations provide insight into overall imaging performance for various conditions. I present general guidelines for maximum incidence angle and field of fiew that provide near diffraction-limited performance. Experimental verification of the MEMS mirrors at 5° and 45° incidence angles validates the analytical results. A Blu-ray optical pick-up imaging demonstration shows the utility of these mirrors for focus control and spherical aberration correction. Imaging results of the first demonstration of a deformable mirror for dynamic agile focus control and spherical aberration correction in a commercial table-top confocal microscope are also shown.
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    A Confocal Microscope and Raman Spectroscopy Probe for Mars exploration
    (Montana State University - Bozeman, College of Engineering, 2002) Crowder, Dawn Michelle
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    Mems 3-D scan mirror for an endoscopic confocal microscope
    (Montana State University - Bozeman, College of Engineering, 2005) Shao, Yuhe; Chairperson, Graduate Committee: David L. Dickensheets.
    Optical MEMS is at a very exciting stage and has become an enabling technology for a variety of applications in telecommunications and high-resolution display and imaging. Among many novel MEMS devices, MEMS scanners and deformable membrane mirrors are especially useful for scanned-beam imaging systems. MEMS scanners are usually used for laser beam scanning. Deformable mirrors provide an approach to modify the optical wavefront adaptively. In optical microsystems, packaging is often a critical part of the system design. Combining functionalities at a single device can reduce complexity of the system. Biaxial beam scanning and focus control are combined together in the MEMS 3-D scan mirror. The mirror surface is made of a goldcoated silicon nitride deformable membrane and works as a positive lens of variable focal length. The membrane sits on a torsional plate that can scan about two orthogonal axes. This architecture is able to move the focus of a laser beam throughout a threedimensional space with a single optical surface. The overall size of the 3-D mirror is 1.5 mm with a usable optical aperture of 0.7 mm. Both the inner and outer scanning axes achieved more than 5o zero-to-peak mechanical scan angles; the deformable membrane achieved a maximum center displacement of more than 3.7 æm, corresponding to an adjustable focal length from infinity to approximately 8 mm. For a confocal laser scanning microscope with illumination wavelength at 500 nm, they provide Nx = Ny = 488 resolvable spots for lateral resolution, and Nz = 32 depth-of-focus distances for depth resolution. To drive the 3-D mirror, the inner axis is operated near resonance (~ 650 Hz); and the outer axis quasi-statically. Operating the outer axis at 2 Hz provides a line resolution of 325 lines/frame at a refresh rate of 2 frames/second. The performance of the 3-D mirror is well matched to the intended application of endoscopic confocal microscopy, and similar devices could prove useful in a variety of optical microsystems needing beam scanning and focus control. This dissertation describes the design, fabrication, characterization, imaging experiment and target applications of the MEMS 3- D scan mirror.
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    Dynamic response of mini cantilever beams in viscous media
    (Montana State University - Bozeman, College of Engineering, 2010) Mishty, Anamika Sharmin; Chairperson, Graduate Committee: Ahsan Mian
    In concurrent engineering, viscosity and density of a fluid are two important parameters as they are the indicators of some predefined standards of the concerned fluids in some specified application. Arguably fluids play an important role in all major engineering applications starting from automobile to biofilm. In this work, we will demonstrate the use of mini cantilever beams for characterization of rheological properties of viscous materials such as lubricating oils. Further miniaturization of the test platform can lead to a MEMS device that can potentially be used for measuring the rheological properties of soft viscoelastic materials such as biofilm. Miniaturization of the measuring instrument is necessary so a small sample volume can be used to perform the test. In this study, the dynamic response of cantilever beams was measured experimentally in air and viscous fluids (e.g. water, and lube oils of three different grades) using a duel channel PolyTec scanning vibrometer. The changes in dynamic response of the beam such as resonant frequency, frequency amplitude, and the Q-factor were compared as functions of the rheological properties (density and viscosity) of fluid media. It may be mentioned here that we used two cantilever beam configurations, one was the plain small stainless steel beam and another was a small stainless steel beam with an aluminum mass attached to it. For both the configurations, the samples were excited by an external shaker at sweeping frequency modes and the beams' motions were recorded by the laser vibrometer focused at different locations of a beam's surface. The reflected signal is directed to a split photo detector whose output is sent to fast-Fourier Transform [FFT] spectrum analyzer.
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    Numerical modeling of the deflection of an electrostatically actuated circular membrane mirror
    (Montana State University - Bozeman, College of Engineering, 2011) Moog, Eric John; Chairperson, Graduate Committee: Steven R. Shaw; David L. Dickensheets (co-chair)
    This thesis outlines a numerical modeling method to describe the deflection behavior and investigate control schemes for an electrostatically actuated deformable membrane mirror, with application to focus control and aberration correction in micrelectromechanical systems. The physics of the membrane are approximated using a finite difference approach with parameters obtained from measurements of a physical device. The model is validated by comparison of simulated and measured mirror position under static and dynamic conditions. This thesis provides simulation results for control schemes that would be difficult or potentially destructive if implemented using real devices. We suggest that the model may be useful for the development of future control strategies and in refining device design. Finally, a number of capacitive sensing circuits are presented as position feedback mechanisms and the capabilities and limitations of each are examined.
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    Analysis and design of mems scan mirrors using periodically stiffened silicon nitride
    (Montana State University - Bozeman, College of Engineering, 2006) Lutzenberger, Bert Jeffrey; Chairperson, Graduate Committee: Robert Oakberg
    This research presents a novel fabrication method combining surface and bulk micromachining techniques to deposit mechanically stiffened silicon nitride films for use in MEMS fabrication. The stiffened silicon nitride film consists of a thin (~1.5 um) top sheet with stiffening fins molded to the back of the film. In the final configuration, the fins extend between 15 um and 40 um vertically from the back of the film. The molded fins are arranged into periodic square and hexagonal cell configurations ranging in size from 10 um to 250 um. The periodic cells significantly increase the bending stiffness of LPCVD silicon nitride films resulting in a film with a high strength-to-weight ratio. Larger aperture, silicon nitride micro mirrors are fabricated with the mechanically stiffened silicon nitride film. The mirrors demonstrate that deformation due to postrelease thermal strain and inertia during dynamic actuation can be mitigated by employing the proposed stiffening technique. Furthermore, the mirrors are fabricated with a minimal amount of processing making the proposed microfabrication technique an attractive solution for various MEMS applications Finally, homogenized material properties are obtained for the periodically stiffened silicon nitride film. The homogenized material properties are then used to simplify finite element models of biaxial and single axis torsion micro mirrors fabricated from the proposed film. The resulting finite element models are shown to be in excellent agreement with the experimental models. The presented numerical analysis method significantly simplifies model complexity while simultaneously reducing the computational cost associated with simulating MEMS built from a periodically stiffened thin film.
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    Surface micro-machined SU-8 2002 deformable membrane mirrors
    (Montana State University - Bozeman, College of Engineering, 2011) Lukes, Sarah Jane; Chairperson, Graduate Committee: David L. Dickensheets
    Imaging systems are continually decreasing in size, especially in applications such as microscopy and cell phone cameras. Much research is being done to increase focus control capabilities of these instruments. This paper describes a wet-etch release and a dry-etch release fabrication technique for SU-8 2002 surface micro-machined deformable mirrors for focus control and compensation of focus-induced spherical aberration. Producing a good quality SU-8 2002 membrane layer proved difficult and a detailed discussion of the recipe development is presented. A thorough review of both release processes is also included. The dry-etch release process has high yield and realizes larger mirrors with greater than a two-fold improvement in stroke, relative to the wet-etch release. This paper presents deflection vs. voltage plots, mechanical frequency response measurements, surface roughness and flatness, and intrinsic stress for the 750 micron - 4.24 mm nominal dimension circular and elliptical boundary membrane mirrors. The use of a 3 mm x 4.24 mm elliptical boundary mirror for 45° incidence focus control in microscopy is also demonstrated. The intrinsic stress of the film indicates that devices of similar size should be capable of 30 micron displacement in the future. This would allow for sufficient focus control in high NA microscopy applications, while the mirror or mechanism for such control could fit into an endoscopic sized imaging system.
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