Determination of the feasibility of using attenuated total reflectance fourier transform-infrared spectroscopy to evaluate thermal ageing of enamel-coated magnet wire

dc.contributor.authorBremer, Philip J.
dc.contributor.authorGeesey, Gill G.
dc.date.accessioned2018-02-01T22:47:01Z
dc.date.available2018-02-01T22:47:01Z
dc.date.issued1997-01
dc.description.abstractA study was initiated to determine the feasibility of employing attenuated total reflectance Fourier transform–infrared spectroscopy (ATR/FT–IR) to detect changes resulting from thermal ageing in the enamel of copper magnet wire. Polyamideimide (SX-81002) was cured on a zinc selenide (ZnSe) internal reflection element (IRE) coated with a thin film of metallic copper. The coated IRE was inserted in a Circle cell housed in a heating jacket and maintained at 250°C on the optical bench of an infrared spectrometer to simulate thermal ageing of enamel-coated magnet wire. Evaluation of the infrared spectra in the fingerprint region suggested that the polymer experienced chemical degradation within a 23 day period of thermal ageing. Through comparisons with controls containing no copper coatings, and ageing studies carried out at 28°C, it was determined that ageing at elevated temperature caused more pronounced chemical changes in the polymer than did exposure to the copper. These results indicate that ATR/FT–IR may be a useful tool to detect enamel fatigue after a short period of thermal ageing.en_US
dc.identifier.citationBremer, P.J. and G. Geesey, “Determination of the Feasibility of Using Attenuated Total Reflectance Fourier Transform-Infrared Spectroscopy to Evaluate Thermal Ageing of Enamel-Coated Magnet Wire,” Journal of Materials Science, 32:141-146 (1997).en_US
dc.identifier.issn0022-2461
dc.identifier.urihttps://scholarworks.montana.edu/handle/1/14290
dc.titleDetermination of the feasibility of using attenuated total reflectance fourier transform-infrared spectroscopy to evaluate thermal ageing of enamel-coated magnet wireen_US
dc.typeArticleen_US
mus.citation.extentfirstpage141en_US
mus.citation.extentlastpage146en_US
mus.citation.issue1en_US
mus.citation.journaltitleJournal of Materials Scienceen_US
mus.citation.volume32en_US
mus.data.thumbpage4en_US
mus.identifier.categoryEngineering & Computer Scienceen_US
mus.identifier.doi10.1023/A:1018539502566en_US
mus.relation.collegeCollege of Engineeringen_US
mus.relation.departmentCenter for Biofilm Engineering.en_US
mus.relation.departmentChemical & Biological Engineering.en_US
mus.relation.departmentChemical Engineering.en_US
mus.relation.researchgroupCenter for Biofilm Engineering.en_US
mus.relation.universityMontana State University - Bozemanen_US

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